The Master Science Graphite Furnace System is an electrothermal atomizer for quantitative trace element analysis by graphite furnace atomic absorption. Connected to a compatible atomic absorption spectrophotometer, it lowers detection limits well below flame AAS, reaching picogram levels for elements such as cadmium.
A nine-step temperature program from ambient to 3000 °C, with adjustable ramp and hold times, lets each method dry, ash and atomize the sample under controlled conditions.
Technical Specifications
Technical data of the Master Science Graphite Furnace System:
- Brand: Master Science
- Model Number: MSGRD-3202SWISS
- SKU: MSGRD-3202SWISS
- Heating Steps: 9
- Temperature Range: 20 °C to 3000 °C (nominal)
- Ramp Time: 0 to 999 s
- Hold Time: 1 to 999 s (ramp + hold ≤ 999 s)
- High-power Heating: 1000 °C to 2700 °C
- Inert Gas: Argon, inlet pressure above 0.3 MPa
- Cooling Water: Tap or recirculated water, at least 2 L/min
- Display: LCD
- Interfaces: AAS spectrophotometer, autosampler, RS232
- Alarms: Gas pressure and furnace overheat
- Characteristic Mass (with AAS): Cd ≤ 1 × 10⁻¹² g; Cu ≤ 1 × 10⁻¹⁰ g
- Power Supply: 220 V ±22 V, 50 Hz ±1 Hz (3 A control; 30 A heating)
- Heating Power: About 5.1 kW at 2700 °C
- Rated Power: 7.2 kW
- Operating Conditions: +10 °C to +30 °C; humidity below 85 %
- Package Dimensions (W × D × H): 730 × 660 × 910 mm
Key Benefits
- Lower detection limits: the Master Science Graphite Furnace System atomizes the whole sample in the tube, reaching picogram levels for trace metals.
- Method flexibility: nine programmable steps with independent ramp and hold times suit dry, ash and atomize stages for different matrices.
- Protected operation: alarms warn of low argon pressure or furnace overheating before damage occurs.
- Easy integration: RS232 and autosampler interfaces connect the furnace to the AAS workflow.
- Small sample volumes: furnace analysis needs far less sample than flame aspiration.
The furnace is designed as an accessory for the Master Science double beam flame AAS analyzer.
Product Features
Temperature Program
- Ambient to 3000 °C nominal range
- Nine heating steps
- Ramp 0 to 999 s and hold 1 to 999 s per step
- High-power heating mode from 1000 °C to 2700 °C
Safety and Utilities
- Argon purge for tube protection
- Water cooling at 2 L/min or more
- Gas pressure and overheat alarms
Connectivity
- Interface to atomic absorption spectrophotometer
- Autosampler connection
- RS232 output and LCD display
Applications
The Master Science Graphite Furnace System is used for trace analysis of:
- Lead, cadmium and other heavy metals in drinking water
- Toxic elements in food and biological samples
- Trace metals in soil and environmental samples
- Impurities in pharmaceutical and high-purity materials
- Research on low-level elemental contamination
Common Laboratory Problems and How This Furnace Helps
Typical trace metal challenges addressed by the Master Science Graphite Furnace System:
- Flame AAS not sensitive enough: furnace atomization reaches far lower concentrations.
- Limited sample volume: microlitre injections are enough for analysis.
- Matrix interference: separate drying and ashing steps remove the matrix before atomization.
- Equipment damage from utility failure: gas and overheat alarms protect the furnace.
- Manual sample injection: an autosampler interface supports unattended runs.